Jon A. Van Loon's Analytical Atomic Absorption Spectroscopy. Selected Methods PDF

By Jon A. Van Loon

Analytical Atomic Absorption Spectroscopy

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A b s o r p t i o n signals a p p e a r in the f o r m of relatively s h a r p p e a k s . P e a k s h a p e for a g i v e n e l e m e n t is influenced b y the c o n d i t i o n of t h e i n s i d e surface of t h e c u p o r b o a t , the p o s i t i o n of t h e c u p o r b o a t in the flame, a n d the n a t u r e of t h e s a m p l e m a t r i x . A r e c o r d e r m u s t b e u s e d w i t h t h e D e l v e s c u p o r s a m p l i n g b o a t s y s t e m s to facilitate d i a g n o s i s of interfer­ ence problems.

Are factors that strongly affect the i n t e r f e r e n c e p a t t e r n . In a test in the a u t h o r ' s l a b o r a t o r y ( 2 0 ) , e v e n w i t h o p e r a t i n g c o n d i t i o n s a d j u s t e d to b e as closely similar as p o s s i b l e , different i n t e r ­ ference p a t t e r n s w e r e o b t a i n e d for m o l y b d e n u m u s i n g t w o different b r a n d s of a t o m i c a b s o r p t i o n e q u i p m e n t . , c o p p e r a n d z i n c , do n o t h a v e s e r i o u s p r o b ­ l e m s a s s o c i a t e d w i t h their d e t e r m i n a t i o n e v e n o v e r a fairly w i d e r a n g e of s a m p l e t y p e s .

To m i n i m i z e i n t e r f e r e n c e s it is often i m p o r t a n t to u s e t h e h i g h e s t - p o w e r r a m p available d u r i n g the a t o m i z a t i o n cycle. W i t h control of t e m p e r a t u r e , this c a n n o w b e d o n e w i t h o u t d a n g e r of o v e r s h o o t i n g the d e s i r e d final t e m p e r a t u r e . W i t h o u t t e m p e r a t u r e c o n - 26 1 GENERAL PRINCIPLES trol c a p a b i l i t y , r e p r o d u c i b l e a n d a c c u r a t e l y definable h e a t i n g cycles w e r e i m p o s s i b l e .

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